US Patent Application for Process and intermediates for
Apr 08, 2003 The solvent was removed on a rotary evaporator and the residue formed was dissolved in 20 mL of EtOAc. This solution was washed with brine and then was dried over anhydrous Na 2 SO 4. Removal of the drying agent followed by evaporation of solvent gave crude optically active diol which was dried under vacuum to provide 1.356 g (quantitative) of ...
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